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polymersource成立于1994年，是一家的高質量建筑控制專業級的聚合物和生物聚合物的研究產品供應商。polymersource的研究團隊包括動態，主管和創新的科學家，在各種學術和研究機構提供*的服務。

polymersource的科學家已經完成了生產3000多嵌段共聚物，產品質量得到了*的認可。除了提供生物/聚合物，聚合物源已經開發了基于我們的產品的合成和應用知識產權。

Sample Name: Poly(butadiene-b-ethylene oxide)

Sample #: P18952-BdEO

(poly butadiene block rich in 1,2-addition)

Structure of 1,2-rich microstructure:

Synthesis Procedure:

Poly(butadiene[1,4- or 1,2 addition]-b-ethylene oxide)

can be prepared by the different routes as reported in the literature (ref: Macromolecules 1996, 29, 6994).

The direct synthesis of diblock copolymer using lithium counter ion in the presence of phosphazene base t-BuP₄ is reported in Macromolecules 1999, 32 (8), 2783–785. The polymers can also be successfully synthesized using the different end-functionalized polymers as investigated in our lab. These methodologies are proprietary.

Characterization:

OH-terminated polybutadiene polymer was analyzed by size exclusion chromatography (SEC) to obtain the molecular weight and polydispersity index (PDI). The final block copolymer composition was calculated from ¹H-NMR spectroscopy by comparing the peak area of the vinylic butadiene protons between about 5.0-5.4 ppm with the ethylene oxide protons at 3.6 ppm. Block copolymer PDI is determined by SEC. Note: The ¹H-NMR of 1,2-polybutadiene is composed of 1 proton signal at 5.4 ppm and 2 proton signals at 5.0 ppm. Signals due to vinylic 1,4-polybutadiene are also present at 5.4 ppm.

Solubility:

Poly(butadiene-b-ethylene oxide) is soluble in THF, CHCl₃, and toluene. The polymer has variable solubility in hexane, methanol, ethanol and water depending on its composition.

DSC thermal analysis of P18952-BdEO:

Thermal analysis of the samples was carried out on a TA Q100 differential scanning calorimeter at a heating rate of 10^oC/min.The midpoint of the slope change of the heat flow plot of the second heating scan was considered as the glass transition temperature (T_g).

The melting temperature (T_m) was taken as the maximum of the endothermic peak where as the crystallization temperature (Tc) was considered as the minimum of the exothermic peak.

貨號	品名	規格	生產廠家
P18952-BdEO	Poly(butadiene(1,2 addition)-b-ethylene oxide)	2g	polymersource

P18952-BdEO現貨供應

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